Abstract：SiC coating was prepared on high-purity graphite using chemical vapor deposition method, and hydrothermal corrosion experiment was conducted to study the relationship between chemical vapor deposition process, coating morphology and structure, and coating hydrothermal corrosion behavior. The results show that with the increase of dilution hydrogen flow rate, the average grain size of the coating decreases, the possibility of free Si appearing in the coating increases, and the resistance to hydrothemal corrosion gradually decreases. As the deposition temperature increases from 1 000 ℃ to 1 300 ℃, the crystallinity and average grain size of the coating first increases and then decreases. The maximum value is obtained at a deposition temperature of 1 200 ℃, and the coating structure and grain morphology remain intact after hydrothermal corrosion. As the temperature of the methyltrichlorosilane water bath increases, the average grain size of the coating increases. The coating prepared at a water bath temperature of 50 ℃ has the worst crystallinity and is the most severely corroded.
毛健, 陈招科, 徐振男, 熊翔. 化学气相沉积SiC涂层的制备及水热腐蚀行为[J]. 粉末冶金材料科学与工程, 2024, 29(5): 373-383.
MAO Jian, CHEN Zhaoke, XU Zhennan, XIONG Xiang. Preparation and hydrothermal corrosion behavior of SiC coating by chemical vapor deposition. Materials Science and Engineering of Powder Metallurgy, 2024, 29(5): 373-383.
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2024, Vol. 29 
