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粉末冶金材料科学与工程  2019, Vol. 24 Issue (3): 248-254    
  工艺技术 本期目录 | 过刊浏览 | 高级检索 |
炭纤维涂层改性对快速制备Cf/SiC复合材料力学性能的影响
孙晔华1, 李国栋1, 叶国柱2, 史琦1, 张洋1, 何岸青2
1. 中南大学 粉末冶金国家重点实验室,长沙 410083;
2. 湖南兴晟新材料科技有限公司,株洲 412000
Effect of carbon fiber coating modification on mechanical properties of rapidly prepared Cf/SiC composite
SUN Yehua1, LI Guodong1, YE Guozhu2, SHI Qi1, ZHANG Yang1, HE Anqing2
1. State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China;
2. Hunan Xingsheng Novel Materials Technology Co., Ltd, Zhuzhou 412000, China
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摘要 以SiC粉末、酚醛树脂粉末及有PyC/SiC复合涂层改性和无涂层改性的两种炭纤维毡/布为原料,采用新型快速成形工艺结合反应熔体浸渗技术制备Cf/SiC复合材料,并对其表面化学气相沉积(chemical vapor deposition(CVD))/SiC涂层。通过XRD物相分析、扫描电镜及复合材料力学性能测试等手段,研究炭纤维涂层改性及表面涂层改性对Cf/SiC复合材料力学性能的影响。结果表明:涂层改性的炭纤维在反应熔渗过程中不被液Si侵蚀,从而提高材料的力学性能;表面CVD SiC涂层改性能够通过填补表面缺陷,包覆易裂部位,涂层脱粘,弥补内部缺陷等方式提高抗弯强度;采用PyC/SiC复合涂层对炭纤维改性后,复合材料抗弯强度由150.90 MPa提高到217.96 MPa,通过表面CVD SiC涂层后,复合材料抗弯强度进一步提高,达到266.94 MPa。
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孙晔华
李国栋
叶国柱
史琦
张洋
何岸青
关键词 Cf/SiC复合材料化学气相沉积界面改性表面改性抗弯强度    
Abstract:Cf/SiC composites were fabricated by new rapid forming process and reactive melt infiltration, using SiC powder, phenolic resin powder and coated as well as uncoated carbon fiber felt/cloth as raw materials. Then the surface of Cf/SiC composites were coated by chemical vapor deposition (CVD) SiC coating. The effects of coating modification of the carbon fiber and surface coating on the mechanical properties of Cf/SiC composite were studied by XRD phase analysis, scanning electron microscopy (SEM) and mechanical properties test of composite. The results show that CVD PyC/SiC composite interface coating can improve the mechanical properties of the composite materials by protecting carbon fibers from liquid Si corrosion during reactive melt infiltration. CVD SiC surface coating can improve the bending strength of Cf/SiC composite by filling surface defects, cladding fragile parts, coating debonding and remedying internal defects. The bending strength of carbon fiber with PyC/SiC composites coating increases from 150.90 MPa to 217.96 MPa. By means of CVD SiC surface coating, the bending strength is further improved to 266.94 MPa.
Key wordsCf/SiC composite    CVD (chemical vapor deposition)    interface coating    surface coating    bending strength
收稿日期: 2018-11-23      出版日期: 2019-07-11
ZTFLH:  TB332  
通讯作者: 李国栋,教授,博士。电话:13087317973;E-mail: lgd63@163.com   
引用本文:   
孙晔华, 李国栋, 叶国柱, 史琦, 张洋, 何岸青. 炭纤维涂层改性对快速制备Cf/SiC复合材料力学性能的影响[J]. 粉末冶金材料科学与工程, 2019, 24(3): 248-254.
SUN Yehua, LI Guodong, YE Guozhu, SHI Qi, ZHANG Yang, HE Anqing. Effect of carbon fiber coating modification on mechanical properties of rapidly prepared Cf/SiC composite. Materials Science and Engineering of Powder Metallurgy, 2019, 24(3): 248-254.
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