Effects of heat treatment on microstructures and mechanical properties of AlSi10Mg alloy produced by selective laser melting
YU Kaibin, LIU Yunzhong, YANG Changyi
National Engineering Research Center of Near-net-shape Forming Technology for Metallic Materials, South China University of Technology, Guangzhou 510640, China
Abstract:AlSi10Mg alloy was prepared by selective laser melting (SLM) process, and then treated by annealing, solid solution and T6 treatment, respectively. The effects of heat treatment on microstructures and mechanical properties of AlSi10Mg alloy produced by SLM were investigated in order to improve heat treatment process of the alloy. The results show that the phases in as-built AlSi10Mg SLM products are α-Al matrix and eutectic Si. The eutectic structure [α-Al+Si] is continuous network distribution on the matrix of α-Al. The sections of both XOY and XOZ have coarse grain, fine crystal and heat affected zones. After annealing treatment, the eutectic Si network is partial dissolution and fracture, the strength decreases and the hardness increases slightly. While after T6 treatment, the eutectic Si appears with scattered and regular geometry inlays in the α-Al matrix, the tensile strength of the alloy decreases, yield strength slightly increases, and ductility significantly increases. In a comprehensive comparison with respect to strength and ductility, the T6 treatment is more suitable for the AlSi10Mg SLM products.
余开斌, 刘允中, 杨长毅. 热处理对选区激光熔化成形AlSi10Mg合金显微组织及力学性能的影响[J]. 粉末冶金材料科学与工程, 2018, 23(3): 298-305.
YU Kaibin, LIU Yunzhong, YANG Changyi. Effects of heat treatment on microstructures and mechanical properties of AlSi10Mg alloy produced by selective laser melting. Materials Science and Engineering of Powder Metallurgy, 2018, 23(3): 298-305.
[1] 赵晓明, 齐元昊, 于全成, 等. AlSi10Mg铝合金3D打印组织与性能研究[J]. 铸造技术, 2016, 37(11): 2402-2404. ZHAO Xiaoming, QI Yuanhao, YU Quancheng, et al.Study on microstructure and mechanical properties of AlSi10Mg alloy produced by 3D printing[J]. Foundry Technology, 2016, 37(11): 2402-2404. [2] KEMPEN K,THIJS L,YASA E, et al.Process optimization and microstructure analysis for selective laser melting of AlSi10Mg[C]// Michael Sealy. Solid Freeform Fabrication Symposium. Texas, USA: KU Leuven Publication, 2011: 22. [3] BRANDL E, HECKENBERGER U, HOLZINGER V, et al.Additive manufactured AlSi10Mg samples using selective laser melting (SLM): Microstructure, high cycle fatigue, and fracture behavior[J]. Materials and Design, 2012, 34(2): 159-169. [4] 张虎, 聂小佳, 朱海红, 等. 激光选区熔化成形高强Al-Cu- Mg合金研究[J]. 中国激光, 2016, 43(5): 78-84. ZHANG Hu, NIE Xiaojia, ZHU Haihong, et al.Study on high strength Al-Cu-Mg alloy fabricated by selective laser melting[J]. Chinese Journal of Lasers, 2016, 43(5): 78-84. [5] MERTENS A, DEDRY O, REUTER D, et al.Thermal treatments of AlSi10Mg processed by laser beam melting[C]// David Bourell. Proceedings of the 26th International Solid Freeform Fabrication Symposium. Austin, USA: The University of Texas at Austin and the Laboratory for Freeform Fabrication, 2015: 1007-1016. [6] 张文奇. AlSi10Mg合金粉末的选区激光熔化成形工艺及性能研究[D]. 武汉: 华中科技大学, 2015: 37-39. ZHANG Wenqi.Investigation on process and performance of AiSi10Mg parts fabricated by selective laser melting[D]. Wuhan: Huazhong University of Science & Technology, 2015: 37-39. [7] 王小军. Al-Si合金的选择性激光熔化工艺参数与性能研究[D]. 北京: 中国地质大学, 2014: 82-102. WANG Xiaojun.Process parameters and properties of selective laser melting Al-Si alloys[D]. Beijing: China University of Geosciences, 2014: 82-102. [8] WEINGARTEN C, BUCHBINDER D, PIRCH N, et al.Formation and reduction of hydrogen porosity during selective laser melting of AlSi10Mg[J]. Journal of Materials Processing Technology, 2015, 221(1): 112-120. [9] THIJS L, KEMPEN K, KRUTH J P, et al.Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder[J]. Acta Materialia, 2013, 61(5): 1809-1819. [10] 袁学兵, 魏青松, 文世峰. 选择性激光熔化AlSi10Mg合金粉末研究[J]. 热加工工艺, 2014, 43(4): 91-94. YUAN Xuebing, WEI Qingsong, WEN Shifeng.Research on selective laser melting AlSi10Mg alloy powder[J]. Hot Working Technology, 2014, 43(4): 91-94. [11] 李卫超, 邹勇志, 曾建民,. 固溶温度和时间对ZL114A合金组织的影响[J]. 机械工程材料, 2008, 32(11): 25-27. LI Weichao, ZOU Yongzhi, ZENG Jianmin.Influence of solution temperature and time on microstructure of ZL114A alloy[J]. Materials for Mechanical Engineering, 2008, 32(11): 25-27. [12] LIU Bingyi, SUN Yu.Effect of heat treatment on microstructure and performance of aluminum-silicon casting alloy[J]. Automobile Technology, 2004(4): 36-39. [13] GU Dongdong, SHEN Yifu.Balling phenomena in direct laser sintering of stainless steel powder: Metallurgical mechanisms and control methods[J]. Materials and Design, 2009, 30(8): 2903-2910. [14] FIOCCHI J, TUISSI A, BASSANI P, et al.Low temperature annealing dedicated to AlSi10Mg selective laser melting products[J]. Journal of Alloys and Compounds, 2017, 695(5): 3402-3409. [15] ZHOU Hua, XIAO Shunhua.Effect of solution treatment on microstructure and mechanical properties of 2E12 aluminum alloy[J]. Aluminum Fabrication, 2011, 25(3): 25-29. [16] 崔忠圻, 覃耀春. 金属学与热处理[M]. 北京: 机械工业出版社, 2007: 382. CUI Zhongqi, TAN Yaochun.Metallography andheat treatment[M]. Beijing: China Machine Press, 2007: 382.