Abstract:321 austenitic stainless steel is widely used in the aerospace and petrochemical industries due to its excellent corrosion resistance. However, conventional manufacturing methods struggle to meet the engineering requirements for the integrated fabrication of its complex structures. In this study, laser powder bed fusion was adopted to fabricate 321 stainless steel. The regulatory laws of laser process parameters on the porosity, formability, and microhardness of the 321 stainless steels were systematically investigated to screen out the optimal forming process parameters. Furthermore, the microstructure, room-temperature tensile properties, and high-cycle fatigue properties of the 321 stainless steels prepared under the optimal parameters were systematically characterized. The results show that the 321 stainless steel fabricated under the optimal process parameters (laser power of 220 W, scanning speed of 800 mm/s, layer thickness of 0.03 mm, and hatch spacing of 0.08 mm) achieves a high relative density of 99.94%. Its microstructure exhibits a typical mixed grain structure composed of columnar and equiaxed grains, with a small amount of retained ferrite (3.5%). The 321 stainless steel possess superior tensile properties, with the yield strength and tensile strength reaching 553 MPa and 662 MPa, respectively, and the elongation being 31.9%. In addition, the fatigue limit of the material attains 530 MPa, and both tensile and fatigue failures follow the ductile fracture mechanism. This study provides an important experimental basis for the process control and engineering service of additively manufactured 321 stainless steel components.
[1] 王招阳, 肖长源, 李昌林, 等. 激光增材制造321不锈钢组织性能研究[J]. 航天制造技术, 2021(3): 19-22. WANG Zhaoyang, XIAO Changyuan, LI Changlin, et al.Microstructure and properties of laser additive manufacturing 321 stainless steel[J]. Aerospace Manufacturing Technology, 2021(3): 19-22. [2] AYAN Y, KAHRAMAN N.Investigation of tensile and fatigue properties of an austenitic stainless steel part fabricated by WAAM[J]. Materials Chemistry and Physics, 2024, 315: 128937. [3] HU S Z, LÜ Y R, LI W M, et al.Linking microstructural evolution to magnetic response for damage assessment in in-service 321 stainless steel[J]. Metals, 2026, 16(2): 134. [4] YIN Q X, CHEN G Q, CAO H, et al.Transformation law of microstructure evolution and mechanical properties of electron beam freeform fabricated 321 austenitic stainless steel[J]. Vacuum, 2021, 194: 110594. [5] 甄隽灏, 徐俊飞, 吴勇华. 金属增材制造缺陷检测技术研究进展[J]. 机械制造, 2025, 63(1): 58-64. ZHEN Junhao, XU Junfei, WU Yonghua.Research progress on defect detection technology of metal additive manufacturing[J]. Machinery, 2025, 63(1): 58-64. [6] JAMBOR M, VOJTEK T, POKORNÝ P, et al.Anomalous fatigue crack propagation behavior in near-threshold region of L-PBF prepared austenitic stainless steel[J]. Materials Science and Engineering A, 2023, 872: 144982. [7] LUO M, CHEN H S, LIAO X Z, et al.Towards in-situ grain boundary engineering in additively manufactured stainless steel 316L via reused powder[J]. Acta Materialia, 2025, 297: 121387. [8] 袁雪婷, 李银山, 臧伟, 等. 2205双相不锈钢在增材制造和热处理过程中组织和力学性能的变化[J]. 焊管, 2023, 46(11): 59-68. YUAN Xueting, LI Yinshan, ZANG Wei, et al.Evolution of microstructure and mechanical properties of 2205 duplex stainless steel during additive manufacturing and heat treatment[J]. Welded Pipe and Tube, 2023, 46(11): 59-68. [9] SARDARIAN S, DEHGAHI S, WEI F, et al.Structured porous 17-PH stainless steel layer fabrication through laser powder bed fusion[J]. International Journal of Sustainable Engineering, 2024, 17(1): 306-321. [10] 梁升翔, 李瑞迪, 袁铁锤, 等. 激光粉末床熔融GH3536合金的显微组织和力学性能[J]. 粉末冶金材料科学与工程, 2025, 30(5): 414-423. LIANG Shengxiang, LI Ruidi, YUAN Tiechui, et al.Microstructure and mechanical properties of GH3536 alloy by laser powder bed fusion[J]. Materials Science and Engineering of Powder Metallurgy, 2025, 30(5): 414-423. [11] 马悦, 袁铁锤, 黄洋, 等. 激光粉末床熔融304L不锈钢显微组织及力学性能各向异性[J]. 粉末冶金材料科学与工程, 2025, 30(4): 364-377. MA Yue, YUAN Tiechui, HUANG Yang, et al.Microstructure and anisotropic mechanical properties of laser powder bed fusion 304L stainless steel[J]. Materials Science and Engineering of Powder Metallurgy, 2025, 30(4): 364-377. [12] 袁晓慧, 李瑞迪, 袁铁锤. Nb含量对激光定向能量沉积Ti-Al-Nb合金组织与力学性能的影响[J]. 粉末冶金材料科学与工程, 2025, 30(3): 204-214. YUAN Xiaohui, LI Ruidi, YUAN Tiechui.Effects of Nb content on microstructure and mechanical properties of Ti-Al-Nb alloys fabricated by laser-directed energy deposition[J]. Materials Science and Engineering of Powder Metallurgy, 2025, 30(3): 204-214. [13] WATRING D S, BENZING J T, HRABE N, et al.Effects of laser-energy density and build orientation on the structure- property relationships in as-built Inconel 718 manufactured by laser powder bed fusion[J]. Additive Manufacturing, 2020, 36: 101425. [14] ZAGADE P R, GAUTHAM B P, DE A, et al.Scaling analysis for rapid estimation of lack of fusion porosity in laser powder bed fusion[J]. Science and Technology of Welding and Joining, 2023, 28(5): 372-380. [15] DEBROY T, WEI H L, ZUBACK J S, et al.Additive manufacturing of metallic components: process, structure and properties[J]. Progress in Materials Science, 2018, 92: 112-224. [16] CHERN A H, NANDWANA P, YUAN T, et al.A review on the fatigue behavior of Ti-6Al-4V fabricated by electron beam melting additive manufacturing[J]. International Journal of Fatigue, 2019, 119: 173-184. [17] ZHANG B, LI Y T, BAI Q.Defect formation mechanisms in selective laser melting: a review[J]. Chinese Journal of Mechanical Engineering, 2017, 30(3): 515-527. [18] XING W, OUYANG D, CHEN Z, et al.Effect of energy density on defect evolution in 3D printed Zr-based metallic glasses by selective laser melting[J]. Science China Physics, Mechanics & Astronomy, 2019, 63(2): 226111. [19] 马成燕, 陶双洋, 韩璐, 等. 激光粉末床熔融技术成形铝合金缺陷研究[J]. 材料科学, 2022, 12(8): 807-814. MA Chengyan, TAO Shuangyang, HAN Lu, et al.Study on the defects of aluminum alloy formed by laser powder bed fusion technology[J]. Material Sciences, 2022, 12(8): 807-814. [20] ZHANG X, XU H, LI Z J, et al.Effect of the scanning strategy on microstructure and mechanical anisotropy of Hastelloy X superalloy produced by laser powder bed fusion[J]. Materials Characterization, 2021, 173: 110951. [21] 吴超群, 胡耀坤, 高建宝, 等. 激光粉末床熔融成形Al-Ce-Ni合金组织性能研究[J]. 有色金属工程, 2024, 14(12): 53-62. WU Chaoqun, HU Yaokun, GAO Jianbao, et al.Microstructure and tensile properties of Al-Ce-Ni alloy produced by laser powder bed fusion[J]. Nonferrous Metals Engineering, 2024, 14(12): 53-62. [22] GHAYOOR M, LEE K, HE Y J, et al.Selective laser melting of 304L stainless steel: role of volumetric energy density on the microstructure, texture and mechanical properties[J]. Additive Manufacturing, 2020, 32: 101011. [23] ASTAFUROV S, ASTAFUROVA E.Phase composition of austenitic stainless steels in additive manufacturing: a review[J]. Metals, 2021, 11(7): 1052. [24] SOFRAS C, ČAPEK J, ARABI-HASHEMI A, et al.Tailored deformation behavior of 304L stainless steel through control of the crystallographic texture with laser-powder bed fusion[J]. Materials & Design, 2022, 219: 110789. [25] KURZYNOWSKI T, GRUBER K, STOPYRA W, et al.Correlation between process parameters, microstructure and properties of 316L stainless steel processed by selective laser melting[J]. Materials Science and Engineering A, 2018, 718: 64-73. [26] STRANTZA M, GANERIWALA R K, CLAUSEN B, et al.Effect of the scanning strategy on the formation of residual stresses in additively manufactured Ti-6Al-4V[J]. Additive Manufacturing, 2021, 45: 102003. [27] ZHANG H Z, XU M T, LIU Z D, et al.Role of local recrystallization behavior on fatigue performance of SLMed 304L austenitic stainless steels[J]. Materials Characterization, 2021, 177: 111159. [28] BADKOOBEH F, MOSTAAN H, RAFIEI M, et al.A study on phase evolutions and tensile-shear performance of dissimilar resistance spot welds formed between AISI 430 ferritic stainless steel and AISI 321 austenitic stainless steel[J]. Journal of Materials Engineering and Performance, 2023, 32(11): 5028-5042. [29] ZHANG M K, LI J W, LIAO X, et al.Influence of cycle number on the compression behavior of nonlinear periodically gradient porous structures produced by laser powder bed fusion[J]. Materials & Design, 2022, 223: 111257. [30] LI S H, ZHAO Y K, KUMAR P, et al.Effect of initial dislocation density on the plastic deformation response of 316L stainless steel manufactured by directed energy deposition[J]. Materials Science and Engineering A, 2022, 851: 143591. [31] JEON J M, PARK J M, YU J H, et al.Effects of microstructure and internal defects on mechanical anisotropy and asymmetry of selective laser-melted 316L austenitic stainless steel[J]. Materials Science and Engineering A, 2019, 763: 138152. [32] WANG J L, YU J, YANG Y X, et al.Study of the remanufacturing critical threshold and remanufacturability evaluation for FV520B-I blade based on fatigue life and FEA[J]. Engineering Failure Analysis, 2020, 112: 104509. [33] MACÍAS J G S, CHEN K W, TANGUY A, et al. High-vacuum laser treatments enhance strength, ductility and fatigue limit of additively manufactured stainless steel[J]. Materials & Design, 2025, 254: 114064. [34] MLIKOTA M, DOGAHE K, SCHMAUDER S, et al.Influence of the grain size on the fatigue initiation life curve[J]. International Journal of Fatigue, 2022, 158: 106562. [35] AGHAYAR Y, BEHVAR A, HAGHSHENAS M, et al.Rotating bending fatigue of laser powder bed fused 316L stainless steel at various stress levels: microstructural evaluation and predictive modeling[J]. Fatigue & Fracture of Engineering Materials & Structures, 2024, 48(2): 783-796.