Quantitative characterization of Inconel 718 alloy powder particle shape and optimization of its SLM forming process
XU Yang1, ZHANG Rong2, XIAO Zhiyu2
1. Nanjing East Precision Machinery Co., Ltd., Nanjing 211100, China; 2. National Engineering Research of Near-Net Sharp Forming for Metallic Materials,South China University of Technology, Guangzhou 510640, China
Abstract:The grain shape of Inconel 718 alloy powder for selective laser melting (SLM) was quantitatively characterized by integrating grain shape parameters. The surface quality, densification behavior, microstructure and mechanical properties of Inconel 718 alloy formed by selective laser melting (SLM) were studied as well. The results show that the overall sphericity of Inconel 718 alloy powder is relatively high. Excessive or deficient volume energy density will lead to obvious nodularization and porosity on the surface of SLM alloy. When the volume energy density is in the range of 120-140 J/mm3, the forming effect of the sample is better. After processed with optimized forming parameters, a large number of directional dendrites form in the deposited sample and the dendrites in molten pool on the side of the sample grow centripetally perpendicular to the boundary. The elongations of specimen at 650 ℃ and room temperature are 1.7 times and 2.6 times higher than these of the standard forging respectively. Although the tensile strength at 650 ℃ is lower than that at room temperature, the elongation of high temperature stretching is 1.5 times that at room temperature.
[1] DECKER R F.The evolution of wrought age-hardenable superalloys[J]. Journal of Metals, 2006, 58: 32-36. [2] 王君. 镍基高温合金在航空发动机中的应用[J]. 中国新通信, 2019, 21(1): 221-222. WANG Jun. Application of nickel-based superalloy in aeroengine[J]. China New Telecommunications, 2019, 21(1): 221-222. [3] RAO G A, KUMAR M, SRINIVAS M, et al.Effect of thermomechanical working on the microstructure and mechanical properties of hot is ostatically pressed superalloy Inconel 718[J]. Materials Science & Engineering A, 2004, 383(2): 201-212. [4] QI H, AZER M, RITTER A.Studies of standard heat treatment effects on microstructure and mechanical properties of laser net shape manufactured Inconel 718[J]. Metallurgical & Materials Transactions Part A, 2009, 40(10): 2410-2422. [5] DEB R T, WEI H L, ZUBACK J S, et al.Additive manufacturing of metallic components-process, structure and properties[J]. Progress in Materials Science, 2018, 92: 112-224. [6] 高正江, 周香林, 李景昊, 等. 增材制造用金属粉末原材料检测技术[J]. 热喷涂技术, 2018(2): 8-14. GAO Zhengjiang, ZHOU Xianglin, LI Jinghao, et al. Testing technologies for metal powder in additive manufacturing[J]. Thermal Spray Technology, 2018(2): 8-14. [7] 杨倩. IN 738合金粉末特性及其选区激光熔化成形性能研究[D]. 兰州: 兰州理工大学, 2019. YANG Qian. Study on the powder characteristics and forming properties in selective laser melting of IN 738 alloy[D]. Lanzhou: Lanzhou University of Technology, 2019. [8] 魏青松, 王黎, 张升, 等. 粉末特性对选择性激光熔化成形不锈钢零件性能的影响研究[J]. 电加工与模具, 2011(4): 52-56. WEI Qingsong, WANG Li, ZHANG Sheng, et al. Study on the effects of power properties on the performance of stainless steel parts produced by selective laser melting[J]. Electromaching & Mould, 2011(4): 52-56. [9] 高超峰, 肖志瑜, 邹海平, 等. 双喷嘴气雾化技术制备球形AlSi10Mg粉末及其表征[J]. 中国有色金属学报, 2019, 29(2): 374-384. GAO Chaofeng, XIAO Zhiyu, ZOU Haiping, et al. Characterization of spherical AlSi10Mg powder produced by double-nozzle gas atomization using different parameters[J]. The Chinese Journal of Nonferrous Metals, 2019, 29(2): 374-384. [10] CARTER L N, ESSA K, ATTALLAH M M.Optimisation of selective laser melting for a high temperature Ni-superalloy[J]. Rapid Prototyping Journal, 2015, 21(4): 423-432. [11] CARTER L N, WANG X, READ N, et al.Process optimisation of selective laser melting using energy density model for nickel-based superalloys[J]. Materials Science & Technology, 2016, 32(7): 1-6. [12] NATALIYA P, JORDAN R, YU S, et al.Optimisation of selective laser melting parameters for the Ni-based superalloy IN-738 LC using Doehlert’s design[J]. Rapid Prototyping Journal, 2017, 23(5): 881-592. [13] CHESTER K W.The shapes of beach pebbles[J]. U.S. Geological Survey Professional Paper, 1923, 131: 75-83. [14] KRUMRETN W.Measurement and geologic significance of shape and roundness of sedimentary particles[J]. Journal of Sedimentary Research, 1941, 11: 64-72. [15] CARTER L N, MARTIN C, WITHERS P J, et al.The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy[J]. Journal of Alloys & Compounds, 2014, 615: 338-347. [16] LIU W, DUPONT J N.Effects of melt-pool geometry on crystal growth and microstructure development in laser surface-melted superalloy single crystals: Mathematical modeling of single- crystal growth in a melt pool (part I)[J]. Acta Materialia, 2004, 52(16): 4833-4847. [17] POPOVICH V A, BORISOV E V, POPOVICH A A, et al.Functionally graded Inconel 718 processed by additive manufacturing: Crystallographic texture, anisotropy of microstructure and mechanical properties[J]. Materials& Design, 2017, 114: 441-449. [18] XING L, SHI J J, WANG C H, et al.Effect of heat treatment on microstructure evolution of Inconel 718 alloy fabricated by selective laser melting[J]. Journal of Alloys & Compounds, 2018, 764: 639-649. [19] DENG D Y, PENG R L, BRODIH H, et al.Microstructure and mechanical properties of Inconel 718 produced by selective laser melting: Sample orientation dependence and effects of post heat treatments[J]. Materials Science & Engineering, A. 2018, 713: 294-306. [20] DAVID S A, VITEK J M, BOATNER L A, et al.Application of single crystals to achieve quantitative understanding of weld microstructures[J]. Materials Science and Technology, 1995, 11(9): 939-948. [21] 牛雯. 热处理对选区激光熔化成形 Inconel 718 合金的组织和性能的影响[D]. 北京: 北京工业大学, 2016. NIU Wen. Effects of heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 super alloy[D]. Beijing: Beijing University of Technology, 2016. [22] 李帅. 激光选区熔化成形镍基高温合金的组织与性能演变基础研究[D]. 武汉: 华中科技大学, 2017. LI Shuai. Fundamental research on the microstructure and properties evolution of nickel-based superalloy fabricated by selective laser melting[D]. Wuhan: Huazhong University of Science and Technology, 2017. [23] SAMES W.Additive manufacturing of Inconel 718 using electron beam melting: Processing, post-processing, & mechanical properties[D]. United States: Texas A & M University, 2015. [24] 冯喆. SLM成形Inconel 718合金显微组织和高温力学性能的研究[D]. 北京: 北京工业大学, 2018. FENG Zhe. Study on the microstructrure and high temperature mechanical properties of Inconel 718 alloy processed by SLM[D]. Beijing: Beijing University of Technology, 2018.