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Preparation and properties of C/C-SiC composites by high-solid-loading slurry impregnation |
YIN Huan, PENG Ke, RAO Fei, YI Maozhong |
State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China |
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Abstract C/C-SiC composites were prepared by high-solid-loading slurry impregnation and densified by precursor infiltration and pyrolysis (PIP) process. The rheological properties of the slurry, the microstructure, the mechanical properties and the ablative properties of the composites were studied. The results show that a good fluidity and permeability high-solid-loading (40%) SiC slurry can be prepared with 5% ethanol water, when the pH value of slurry is 6 and the mass fraction of PEI is 0.7%. SiC mainly concentrates in the fiber webs between the non-woven layers homogeneously. The bending strength and fracture toughness of C/C-SiC composites are 335.7 MPa and 16.2 MPa·m1/2, respectively. C/C-SiC composites have good ablation resistance at 2 000 ℃, and the oxidation product SiO2 can fill the defects such as pores and cracks to prevent the further oxidation of the materials.
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Received: 13 March 2018
Published: 12 July 2019
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