高纯铼及其化合物的制备与应用研究进展

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Abstract Rhenium has excellent properties such as high temperature resistance and corrosion resistance, and is widely used in high temperature alloys, aerospace special alloys, petrochemicals and other fields. This article introduces various preparation techniques of high-purity rhenium and its compounds, analyzes the advantages and disadvantages of preparing high-purity ammonium perrhenate by precipitation crystallization, ion exchange, and solvent etraction and its application sitiation, and discusses the research progress of preparing high-purity rhenium powder by hydrogen reduction, plasma, electrolysis, and vapor deposition. The application prospects of rhenium in the field of alloys are outlined.

Key words： ammonium perrhenate high purity rhenium rhenium alloy preparation application

Received: 15 May 2020 Published: 18 September 2020

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	ZHANG Jiarun
	LIU Zhiyong
	LIU Zhihong
	LI Qihou

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ZHANG Jiarun,LIU Zhiyong,LIU Zhihong, et al. Research progress on preparation and application of high-purity rhenium and its compounds[J]. Materials Science and Engineering of Powder Metallurgy, 2020, 25(4): 273-279.

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http://pmbjb.csu.edu.cn/EN/ OR http://pmbjb.csu.edu.cn/EN/Y2020/V25/I4/273

[1] 刘世友. 铼的应用现状与展望[J]. 稀有金属与硬质合金, 2000(1): 57-60.
LIU Shiyou.Current situation and prospect of rhenium application[J]. Rare Metals and Cemented Carbides, 2000(1): 57-60.
[2] SABISCH J E C, MINOR A M. Microstructural evolution of rhenium Part I: Compression[J]. Materials Science and Engineering A, 2018, 732: 251-258.
[3] WANG Y, WANG C Y.Recent advances of rhenium separation and enrichment in China: Industrial processes and laboratory trials[J]. Chinese Chemical Letters, 2018, 29(3): 345-352.
[4] NIKONOVA O A, CAPRON M, FANG G, et al.Novel approach to rhenium oxide catalysts for selective oxidation of methanol to DMM[J]. Journal of Catalysis, 2011, 279(2): 310-318.
[5] JIN S, SEO B B, JAHED Z, et al.Fabrication and mechanical properties of sub-micron nanocrystalline rhenium-nickel alloy pillars[J]. Materials Letters, 2015, 149: 113-115.
[6] XIONG Y, SONG Y, TONG Q, et al.Adsorption-controlled preparation of anionic imprinted amino-functionalization chitosan for recognizing rhenium(VII)[J]. Separation and Purification Technology, 2017, 177: 142-151.
[7] 吴贤, 李来平, 张文钲, 等. 铼的性质及铼资源分布[J]. 矿业快报, 2008, 24(11): 67-69.
WU Xian, LI Laiping, ZHANG Wenzheng, et al.Rhenium properties and rhenium resource distribution[J]. Express Information of Mining Industry, 2008, 24(11): 67-69.
[8] MAMO S K, ELIE M, BARON M G, et al.Leaching kinetics, separation, and recovery of rhenium and component metals from CMSX-4 superalloys using hydrometallurgical processes[J]. Separation and Purification Technology, 2019, 212: 150-160.
[9] HORI H, OTSU T, YASUKAWA T, et al.Recovery of rhenium from aqueous mixed metal solutions by selective precipitation: A photochemical approach[J]. Hydrometallurgy, 2019, 183: 151-158.
[10] VOSOUGH M, SHAHTAHMASEBI N, BEHDANI M.Recovery rhenium from roasted dust through super para-magnetic nano-particles[J]. International Journal of Refractory Metals and Hard Materials, 2016, 60: 125-130.
[11] 张德尧. 铼资源及其应用[J]. 稀有金属快报, 2002(2): 15-16.
ZHANG Deyao.Rhenium resources and applications[J]. Rare Metals Letters, 2002(2): 15-16.
[12] KESIEME U, CHRYSANTHOU A, CATULLI M.Assessment of supply interruption of rhenium, recycling, processing sources and technologies[J]. International Journal of Refractory Metals and Hard Materials, 2019, 82: 150-158.
[13] LESSARD J D, GRIBBIN D G, SHEKHTER L N.Recovery of rhenium from molybdenum and copper concentrates during the looping sulfide oxidation process[J]. International Journal of Refractory Metals and Hard Materials, 2014, 44(3): 1-6.
[14] 郭株辉, 沈裕军, 冯洁. 从某铜矿伴生铼所产低等品中提取高纯铼酸铵的技术研究[J]. 中国钼业, 2015(4): 31-35.
GUO Zhuhui, SHEN Yujun, FENG Jie.Study on the technology of extracting high purity ammonium rhenate from low levels of rhenium associated with a copper mine[J]. China Molybdenum Industry, 2015(4): 31-35.
[15] GAETE J, MOLINA L, ALFARO I, et al.Recovery and separation of rhenium and molybdenum from aqueous solutions that simulate mine waters using magnetite nanoparticles functionalized with amine-derivative groups[J]. Minerals Engineering, 2019, 136: 66-76.
[16] QUIJADA-MALDONADO E, ALLAIN A, PÉREZ B, et al. Selective liquid-liquid extraction of molybdenum (VI) and rhenium (VII) from a synthetic pregnant leach solution: Comparison between extractants and diluents[J]. Minerals Engineering, 2020, 145: 106060.
[17] 杜国山, 李少华, 邱爽. 钼精矿多膛炉焙烧烟气中铼的回收[J]. 矿冶工程, 2015, 24(z1): 132-134,137.
DU Guoshan, LI Shaohua, QIU Shuang.Recovery of rhenium from roasting flue gas of molybdenum concentrate multi-chamber furnace[J]. Mining and Metallurgical Engineering, 2015, 24(z1): 132-134, 137.
[18] 周宇飞. 高纯铼酸铵制取工艺研究[J]. 铜业工程, 2016(6): 56-59.
ZHOU Yufei.Study on the preparation technology of high purity ammonium rhenate[J]. Copper Engineering, 2016(6): 56-59.
[19] 王心一, 彭应钦, 王鑫, 等. 废弃物中铼的提取方法与回收应用研究[J]. 辽宁化工, 2019, 48(5): 411-414.
WANG Xinyi, PENG Yingqin, WANG Xin, et al.Study on rhenium extraction and recovery from waste materials[J]. Liaoning Chemical Industry, 2019, 48(5): 411-414.
[20] ZHANG B, LIU H, WANG W, et al.Recovery of rhenium from copper leach solutions using ion exchange with weak base resins[J]. Hydrometallurgy, 2017, 173: 50-56.
[21] 秦玉楠. 离子交换法提取铼酸铵新工艺[J]. 中国钼业, 1998(5): 39-41.
QING Yunan.A new technology for the extraction of ammonium rhenate by ion exchange[J]. China Molybdenum Industry, 1998(5): 39-41.
[22] 陈昆昆, 操齐高, 张卜升, 等. 高温合金酸浸液回收高纯铼酸铵试验研究[J]. 有色金属(冶炼部分), 2019(9): 45-48.
CHEN Kunkun, CAO Qigao, ZHANG Busheng, et al.Study on recovery of high purity ammonium rhenate from acid leaching of superalloy[J]. Nonferrous Metals (Extraction Metallurgy), 2019(9): 45-48.
[23] LESZCZYŃSKA-SEJDA K, MAJEWSKI T, BENKE G, et al. Production of high-purity ammonium perrhenate for W-Re-Ni-Fe heavy alloys[J]. Journal of Alloys and Compounds, 2012, 513: 347-352.
[24] NEBEKER N, HISKEY J B. Recovery of rhenium from copper leach solution by ion exchange[J]. Hydrometallurgy, 2012, 125/126: 64-68.
[25] 王丹. 溶剂萃取法富集铼的研究[D]. 郑州: 郑州大学, 2016: 68.
WANG Dan.Study on enrichment of rhenium by solvent extraction[D]. Zhengzhou: Zhengzhou University, 2016: 68.
[26] CHEEMA H A, ILYAS S, MASUD S, et al.Selective recovery of rhenium from molybdenite flue-dust leach liquor using solvent extraction with TBP[J]. Separation and Purification Technology, 2018, 191: 116-121.
[27] PETROVA A M, KASIKOV A G.Rhenium (VII) solvent extraction with mixtures of tertiary amine and oxygen-containing extractants from sulphate media[J]. Hydrometallurgy, 2016, 165: 270-274.
[28] SRIVASTAVA R R, KIM M S, LEE J C, et al.Liquid-liquid extraction of rhenium(VII) from an acidic chloride solution using Cyanex 923[J]. Hydrometallurgy, 2015, 157: 33-38.
[29] CAO Z F,ZHONG H, QIU Z H .Solvent extraction of rhenium from molybdenum in alkaline solution[J]. Hydrometallurgy, 2009, 97(3): 153-157.
[30] 钱勇. 溶剂萃取法制取铼酸铵[J]. 铜业工程, 2004(3): 26-28.
QIAN Yong.Preparation of ammonium rhenate by solvent extraction[J]. Copper Engineering, 2004(3): 26-28.
[31] 邹振球, 周勤俭. 钼精矿石灰焙烧-N235萃取工艺提取钼铼[J]. 矿冶工程, 2002, 22(1): 79-81, 84.
ZOU Zhenqiu, ZHOU Qinjian.Extraction of molybdenum and rhenium from molybdenum concentrate by lime roasting-N235 extraction process[J]. Mining and Metallurgical Engineering, 2002, 22(1): 79-81, 84.
[32] KIM H S, PARK J S, SEO S Y, et al.Recovery of rhenium from a molybdenite roaster fume as high purity ammonium perrhenate[J]. Hydrometallurgy, 2015, 156: 158-164.
[33] SALEHI H, TAVAKOLI H, ABOUTALEBI M R, et al.Recovery of molybdenum and rhenium in scrub liquors of fumes and dusts from roasting molybdenite concentrates[J]. Hydrometallurgy, 2019, 185: 142-148.
[34] HONG T, LIU M B, MA J, et al.Selective recovery of Rhenium from industrial leach solutions by synergistic solvent extraction[J]. Separation and Purification Technology, 2020, 236: 116281.
[35] 李玉萍, 李莉芬, 王献科. 液膜法提取高纯铼[J]. 中国钼业, 2001, 25(6): 23-26.
LI Yuping, LI Lifen, WANG Xianke.Extraction of rhenium by liquid membrane method[J]. China Molybdenum Industry, 2001, 25(6): 23-26.
[36] 申友元, 易晓明, 廖彬彬, 等. 一种高纯铼粉的制备方法: 中国, 02114247.5[P].2002-07-08.
SHEN Youyuan, YI Xiaoming, LIAO Binbin, et al. A preparation method of high purity rhenium powder: China, 02114247.5[P].2002-07-08.
[37] 刘红江, 李瑞迪, 周霞, 等. 一种高纯铼粉的制备方法: 中国, 201710234499.6[P].2017-04-12.
LIU Hongjiang, LI Ruidi, ZHOU Xia, et al. A preparation method of high purity rhenium powder: China, 201710234499.6[P].2017-04- 12.
[38] 范兴祥, 余宇楠, 张凤霞. 一种从含铼高砷铜硫化物中制备高纯铼粉的方法: 中国, 105983707 A[P].2015-01-27.
FAN Xingxiang, YU Yunan, ZHANG Fengxia. A method of preparing high purity rhenium powder from high arsenic copper sulfide containing rhenium: China, 105983707 A[P].2015-01-27.
[39] 孙元, 周亦胄, 候桂臣, 等. 一种超高纯铼锭的制备方法: 中国, 201711144590.5[P].2017-11-17.
SUN Yuan, ZHOU Yizhou, HOU Guichen, et al. A method for the preparation of ultra-high purity rhenium ingot: China, 201711144590. 5[P].2017-11-17.
[40] YE L G, OUYANG Z, CHEN Y M, et al.Recovery of rhenium from tungsten-rhenium wire by alkali fusion in KOH-K₂CO₃ binary molten salt[J]. International Journal of Refractory Metals and Hard Materials, 2020, 87: 105148.
[41] 周令治,陈少纯. 稀散金属提取冶金[M]. 北京: 冶金工业出版社, 2008: 331-333.
ZHOU Lingzhi, CHEN Shaochun.Rare Metal Extraction Metallurgy[M]. Beijing: Metallurgy Industry Press, 2008: 331-333.
[42] HUANG Q, LYONS T W.Electrodeposition of rhenium with suppressed hydrogen evolution from water-in-salt electrolyte[J]. Electrochemistry Communications, 2018, 93: 53-56.
[43] RIVERA J G, GARCIA-GARCIA R, COUTINO-GONZALEZ E, et al.Hydrogen evolution reaction on metallic rhenium in acid media with or without methanol[J]. International Journal of Hydrogen Energy, 2019, 44(50): 27472-27482.
[44] 周乐君. 化学气相沉积法制备超细铼粉的研究[D]. 长沙: 中南大学, 2010: 60.
ZHOU Lejun.Study on the preparation of ultrafine rhenium powder by chemical vapor deposition[D]. Changsha: Central South University, 2010: 60.
[45] JUREWICZ J W, GUO J. Process for plasma synthesis of rhenium nano and micro powders,for coatings and near net shape deposits thereof and apparatus there for: US, 2005/0211018A1[P]. 2005-09-29.
[46] 黄劲松, 周继承, 刘文胜, 等. 高密度合金粉末的制备与处理[J]. 稀有金属与硬质合金, 2003, 31(4): 40-44.
HUANG Jingsong, ZHOU Jicheng, LIU Wensheng, et al.Preparation and treatment of high density alloy powder[J]. Rare Metals and Cemented Carbides, 2003, 31(4): 40-44.
[47] 张英明. 生产铼部件的电子束物理气相沉积法[J]. 稀有金属快报, 2003(4): 20-21.
ZHANG Yingmeng.Electron beam physical vapor deposition method for rhenium components[J]. Rare Metals Letters, 2003(4): 20-21.
[48] YANG S R, TAN C W, YU X D, et al.A study of CVD growth kinetics and morphological evolution of rhenium from ReCl₅[J]. Surface and Coatings Technology, 2015, 265: 38-45.
[49] TUFFIAS R, KAPLAN R, WILLIAMS B, et al.Iridium/rhenium combustion chambers-From concept to reality[C]// IANNOTTA B. Space Programs & Technologies Conference. Huntsville, US: American Institute of Aeronautics and Astronautics, 2013: 685-692.
[50] 王海哲. CVD铼的工艺及性能研究[D] .长沙: 国防科技大学, 2005: 62.
WANG Haizhe.Study on the process and properties of CVD rhenium[D]. Changsha: National University of Defense Technology, 2005: 62.
[51] HELBIG T, GILBRICHT S, LEHMANN F, et al.Oxidative leaching of a sulfidic flue dust of former copper shale processing with focus on rhenium[J]. Minerals Engineering, 2018, 128: 168-178.
[52] LAN X, LIANG S, SONG Y.Recovery of rhenium from molybdenite calcine by a resin-in-pulp process[J]. Hydrometallurgy, 2006, 82(3): 133-136.
[53] SUNH, YU J J, LI G H, et al. Co-volatilizing-water leaching process for efficient utilization of rhenium-bearing molybdenite concentrate[J]. Hydrometallurgy, 2020, 192: 105284.
[54] 谭拴斌, 郭让民, 杨升红, 等. 钼铼合金的结构和性能[J]. 稀有金属, 2003, 27(6): 788-793.
TAN Shuanbin, GUO Rangmin, YANG Shenghong, et al.Structure and properties of Mo-Re alloy[J]. Rare Metals Letters, 2003, 27(6): 788-793.
[55] 王广达, 刘国辉, 熊宁. 一种钼铼合金管材的制备方法: 中国, 201711423154.1[P].2017-12-25.
WANG Guangda, LIU Guohui, XIONG Ning. A preparation method of Mo-Re alloy pipe:China,201711423154.1[P].2017-12-25.
[56] MORITO F.Characteristics of EB-weldable molybdenum and Mo-Re alloys[J]. Jom, 1993, 45(6): 54-58.
[57] MANNHEIM R L,GARINJ L.Strain hardening of rhenium and two typical molybdenum-rhenium alloys manufactured by powder sintering[J]. Zeitschrift Fuer Metallkunde, 2000, 91(10): 848-853.
[58] 何浩然, 刘奇, 王志鹏, 等. 钨铼合金制备及应用[J]. 工业计量, 2015, 25(5): 24-27.
HE Haoran, LIU Qi, WANG Zhipeng, et al.Preparation and application of W-Re alloy[J]. Industrial Measurement, 2015, 25(5): 24-27.
[59] 宋琳, 蔡靖宇, 桂锦莹. 钨铼合金粉末冶金过程若干问题的初步研究[J]. 上海钢研, 1978(3): 3-20, 55.
SONG Lin, CAI Jingyu, GUI Jinying.Preliminary study on some problems in P/M process of W-Re alloy[J]. Journal of Shanghai Iron and Steel Research, 1978(3): 3-20, 55.
[60] 姜山, 陈巧旺, 姜中涛, 等. 一种硬度高的钨钽铼合金的制备方法:中国, 201910026643.6[P].2019-01-11.
JIANG Shan, CHEN Qiaowang, JIANG Zhongtao, et al. A preparation method of tungsten tantalum rhenium alloy with high hardness: China, 201910026643.6[P].2019-01-11.