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Effectts of heat treatment process on microstructure and mechanical property of IN713C alloy prepared by injection molding |
XIE Xiaohui1, WU Wei1, PAN Donghua1, YANG Zhongchen2, LU Renwei2, LI Duxin1 |
1. State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China; 2. Changsha Juzhong Metallurgy Technology Co., Ltd., Changsha 410000, China |
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Abstract IN713C alloy was prepared through metal injection molding using IN713C pre-alloyed gas atomized powder as raw powder, after solution treatment at 1 150, 1 175 and 1 120 ℃, and then aging at 760, 850 and 930 ℃. The microstructure and phase composition of the alloy were observed and analyzed by scanning electron microscopy (SEM) and energy spectrometer. The hardness and tensile strength of the alloy in temper state were determined. The results show that the γ′ precipitation phase in cooling phase decreases when the solution temperature continue to increase over a certain value. The hardness and tensile strength of the alloy reaches to 42.4 HRC and 1 175.9 MPa respectively when solid solution at 1 175 ℃. When aging at 760 ℃, the hardness and tensile strength reaches 43.6HRC and 1 223.7MPa respectively. When the aging temperature is above 760 ℃, γ′ phase size become coarser due to larger lattice mismatch; with increasing aging treatment temperature, γ′ phase the size increases, the quantity of γ′ phase and the volume fraction of the strengthening phase decrease, and the hardness and tensile strength of the alloy decrease. The optimal heat treatment process of IN713C in this study is 1 175 ℃2 h/AC+760 ℃16 h/AC.
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Received: 27 March 2017
Published: 11 July 2019
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[1] 金狂浩, 陈康华, 祝昌军, 等. 硬质合金基体对涂层刀具高速切削镍基高温合金切削性能的影响[J]. 粉末冶金材料科学与工程, 2012, 17(4): 437-443. JIN Kuanghao, CHEN Kanghua, ZHU Changjun, et al, Effects of cemented carbide substrates on tool cutting performance in high-speed machining nickel-based superalloy[J]. Materials Science and Engineering of Powder Metallurgy, 2012, 17(4): 437-443. [2] 张志伟, 牛永吉, 史世凤, 等. Inconel713C合金研究现状[J].金属材料研究, 2014(4): 17-22. ZHANG Zhiwei, NIU Yonji, SHI Shifeng, et al.Development of Inconel713C super alloy[J]. Research on Metallic Materials, 2014(4): 17-22. [3] 候介山, 郭建亭, 周兰章, 等. K44镍基高温合金长期时效过程中γ′粗化对拉伸性能的影响[J]. 金属学报, 2006, 42(5): 481-486. HOU Jieshan, GUO Jianting, ZHOU Lanzhang, et al.Effects of γ-precipitate coaesening on tensile properties of Ni base superalloy K44 during long-term aging[J]. Acta Metallrugica Sinica, 2006, 42(5): 481-486. [4] 罗学军, 王晓峰, 马国君, 等. 热处理对FGH95合金组织和性能的影响研究[J]. 粉末冶金技术, 2012, 30(1): 12-17. LUO Xuejun, WANG Xiaofeng, MA Guojun, et al.Effect of heat treatment on microstructure and properties of FGH95 alloy[J]. Powder Metallurgy Technology, 2012, 30(1): 12-17. [5] KERN A, BLÖMACHER M, TERMAAT J, et al. MIM superalloys for automotive applications[C]// Proc PM2010 World Congress-Powder Injection Moulding Super Alloys & Composites. Shrewsbury, UK. 2010: 383-390. [6] 吴谓, 李笃信, 杨文彦, 等. 金属注射成形制备IN713C合金的研究[J]. 粉末冶金工业, 2017, 27(2): 1-5. WU Wei, LI Duxin, YANG Wenyan, et al.Preparation of injection molded IN713C alloy[J]. Powder Metallurgy Industry, 2017, 27(2): 1-5. [7] GES A, PALACIO H, VERSACI R.IN-713C characteristic properties optimized through different heat treatments[J]. Journal of Materials Science, 1994, 29(13): 3572-3576. [8] 刘伯操, 全宏声, 邢致信. 航空材料应用手册[M]. 北京: 北京航空材料研究院, 1996: 98-200. LIU Bocao, QUAN Hongsheng, XING Zhixin.Handbook of Aeronautical Materials Applications[M]. Bejing: Beijing Institute of Aerial Materials, 1996: 98-200. [9] GEROLD V, HABERKORN H.On the critical resolved shear stress of solid solutions containing coherent precipitates[J]. Physica Status Solidi, 1966, 16(2): 675-684. [10] MANIAR G N, BRIDGE J E.Effect of gamma-gamma prime mismatch, volume fraction gamma prime, and gamma prime morphology on elevated temperature properties of Ni, 20 Cr, 5.5 Mo, Ti, Al alloys[J]. Metallurgical Transactions, 1971, 2(1): 95-102. |
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